简介：ThesynthesisofanewtypeofX-ray-sensitivecompound'di-(1-hydroxylundecyl)diselenide'anditsapplicationinthepreparationofanewtypeofliposomewithX-raysensitivitywasreported.Thisnewliposomewassynthesizedtoencapsulatedoxorubicinhydrochloride(Dox),withitsphysicalandchemicalproperties,stability,andradiationsensitivitydetermined.BasedonthepH-gradientmethod,liposomalDoxwaspreparedviaultrasonicemulsificationandthenpurifiedonaSephadexG50mini-column.UVspectrophotometryandliquidchromatographywereusedtodetecttheencapsulationefficiencyandradiationsensitivityoftheDox-loadedliposome.Theresultsshowthatthroughchangesinreleaserate,thisliposomeshowsarelativeradiosensitivity.Intermsofradiationsensitivity,thedrugleakrateoftheX-ray-sensitiveDox-loadedliposomeincreasedgraduallyandpeakedat65.4%undertheX-rayradiationofadoseof10Gyormorethan10Gy,whichissignificantlydifferentfromthatofordinaryliposomes.Meanwhile,X-ray-sensitiveDox-loadedliposomehasagooddispersionstability,withanaverageparticlesizeofapproximate120nm.TheefficiencyofthisliposomeencapsulatingDoxwas75.84%,slightlylowerthanthatofordinaryliposomes.TheX-ray-sensitiveDox-loadedliposomeexhibitedsuspensionstabilitywithin30dofstorageat4°C,withoutvisibleprecipitation.Di-(1-hydroxylundecyl)diselenideissafeandnoncytotoxicandcomparedwiththoseofsyntheticphospholipidsitssynthesisislowcostanddoesnotrequirecomplexconditions.

简介：InordertoexplorethefeasibilityofusingX-raytomeasuremoisturecontentinthedryingprocessandhaveafurtherstudyontheeffectofprecisionofmoisturecontentwhenscanningthroughdifferentgraindirections,X-rayscanningmethodandweightingmethodwereusedtomeasureaveragemoisturecontentofCunninghamialanceolataduringhotairdrying.Theresultsshowthatthemoisturecontentvaluesoftwomethodswereveryclosetooneanother,thedeterminationcoefficientsofbothwerehighlycorrelatedwithavalueover0.99,andtheabsolutedeviationwasbelow2%;whenscanningalongradialdirectionandlongitudinaldirection,theprecisionsofaveragemoisturecontentwerehigherthanthatofthetangentialdirection,butthedeviationcanbenegligibleintheactualmeasurement;inthepracticalapplication,theeffectofgraindirectiononprecisionofmoisturecontentmeasurementcouldnotbetakenintoaccountwhenusingX-raytomeasurethemoisturedistributionofwood.

简介：X-rayThomsonscatteringtechniquefordiagnosingdenseplasmawasdemonstratedonShenguang-Πlaserfacility.Laserplasmax-raysourceoftitaniumHe-αlines(～4.75keV),generatedbylaserbeam(1.5kJ/527nm/2ns)heatedtitaniumthinfoil,wasusedasx-rayprobebeam.Thex-rayprobewasthenscatteredbycoldCHfoamcolumnof1g/cm3density.Thescatteredradiationat90wasdiffractedbypolyethyleneterephthalate(PET)crystalandrecordedonx-raycharge-coupleddevice.Well-definedscatteringspectrawereobtainedwithgoodsignaltonoiseratio.

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简介：TheagingbehaviorofAl-Cu-Mg-AgalloyswithhighCu/Mgwasstudiedbytransmissionelectronmicroscopy(TEM)andsmall-angleX-rayscattering(SAXS)usingsynchrotronradiation.TEMstudyrevealsthatthemajorstrengtheningphasesofthealloyafteragingat160?Cfor10hareΩandlessθ′.SAXSstudyshowsthatthescatteringpatternsarecomposedofseveralconcentriccirclesatthebeginningofagingprocess,whichisreplacedbythebutterfly-wingsscatteringpatternswiththeincreaseofagingtime...