简介：ThecyclicvoltammetryandpotentiostaticelectrolysiswereusedtoinvestigatethepreparingofDy-BialloyfilmsinLiCl-DMSO(dimethylsulfoxide)system.Theeffectsofseveralfactorsincludingthepotentialofdeposition,concentrationsofmainsalts,andtheconcentrationratioofDyCl3toBi(NO3)3werestudied.Dy-Bialloyfilmscontaining4.82%-80.62%(massfraction)dysprosiumwerepreparedinDyCl3-Bi(NO3)3-LiCl-DMSOsystembycontrollingthesystemcompositionanddepositionconditions.Thefilmsaregray,uniform,metalliclusterandadherefirmlytothecoppersubstratesanalyzedbySEM(scanningelectronmicroscope),EDS(X-rayenergydispersiveanalysis),andXRD(X-raydiffraction).Afterheattreatmentat718Kforlh,thealloyphaseofDy-BiwasfoundinXRDpatterns.